|
玻璃漏斗 Glass funnel long stem e5E_;MvL, " k0 G" f8 Z, _* Z# ?" R
试管 test tube test tube brush test tube holder test tube rack GVV"Vfc * p N3 X# P4 B0 I
蒸发皿 evaporating dish small YP[eW*<* ( y$ P' H% t$ _3 S
烧杯 beaker x R`_>L , U H& _. X9 b* w. b) o6 y) J
锥形瓶 Erlenmeyer Nx \KCa
/ r+ Z& I9 d0 c* g量筒 grad cylinder kQG@V<1 ( W. c/ D9 w8 O2 `) E
洗瓶 plastic wash bottle ScCw7M+6<< 8 q/ c2 ]4 ?6 ~
勺皿 casserole ,small eO~--Wf[
0 B1 P7 G, L5 U" ]stoppered flask ;~ SEeOF'
4 j9 M: A* b: Q9 [- J分液漏斗 separalory funnel xp{!fC#
/ e4 O( V/ `+ z$ G6 t" P4 S+ w: ?water bath/oil bath Q)A\c~ l@;
6 u* l0 ~% }/ B. Z/ J; tstrring bar e'/ <mo f * _9 Y8 q2 E6 C. z2 D! E# E7 S
magnetic stirrer D-UU^_(uB
2 L! n) F$ Z* W8 w) U1 c$ `冷凝器 condenser >-|;m&F
$ g# G0 e4 Q4 }, p# [7 |" i# M) rBallast bottle o v\ In. + |' w' r. N- m* q. D1 X# q2 U
圆颈烧瓶 Round-buttom flask z6u>3klm> + G4 C. s E: g' @
试剂瓶 reagent bottles X7u0=\ k}
' X3 r; |; _7 ?4 ]托盘天平 platform balance 台秤 x?.mp+
% \9 c, D% |- g: \- d0.1g 托盘pan 指针刻度表pointer and scale \)IchC 0
, g+ h- j3 I5 |" P) q8 ^6 x4 s" hcrossbeams and sliding weights 游码 dx 24 o7.
- s& q; t# A; [" F: v分析天平 two-pan/single-pan analytical balance WE?ldO< / Y l4 {: o. {: Q7 o- {
滴定管 burette glass bead(basic) nozzle sb$N1ufg5d
7 V9 w& A. I' i3 `* f7 Q移液管 pipette 胖肚 elongated glass bulb 2Z@:XAU-p
3 N4 t0 I8 C3 @& a) a0 [: T洗耳球 rubber suction bulb sm;Y[TuAH # l! ?. ~; A- p! ~
玻棒 glass rod /aQQ z9 * F; z5 `. G7 K; ^( a' T1 E; m
玻璃活塞 stopcock Y*7awPNo
- q: y, Z1 f- }; A容量瓶 pyknowmeter flasks p={WE:4$M& $ D, L* L- B3 C x1 I
比重瓶 (one-mark)volumetric flasks k/2VOZ % a9 w9 f. N# t- A! w; _
}Q%wt_H $ T5 `$ r9 [: N A
胖肚吸管 one-mark pipette q!'qf: >
' h/ B& i9 [# m2 N( z) M$ N* h9 L刻度吸管 graduated pipettes mpiGVXfj " M7 J6 |$ o, v; g. m) R+ s
实验仪器清单 $7P4j6#(
9 i5 U Z4 g8 }: _0 E0 ]0kVGUM
+ w6 F3 q2 u. P# I4 X( T% {1、 柜子中 四、抽屉中: fIR~Jy S , {3 b2 Z) P4 N9 |% L3 Y
锥形瓶(conical flask) 250ml×4 药匙(medicine spoon)×1 KyI/.A< - l! ?7 n0 q6 T. E1 s
(Erlenmeyer flask) 100 ml×3 滴管(drip tube;dropper)×2 Wof:[BhO
9 \% X: F# }7 h `' P烧杯(beaker) 500 ml×1 玻棒(Glass stic)×2 t'6}et
: k' _1 O# |7 h' m n6 X" _3 S/ T250 ml×3 木试管夹(test tube clamp;test tube holder)×1 ;<fw>`:2
) i6 t4 k8 _3 }& F100 ml×3 胖肚吸管(straws) 25 ml×1 Yl]]o . 5 L6 B( o' h2 s2 {
50 ml×2 10 ml×1 JWE J? & e3 E. Y7 o- ?# k& h( N" M! P
容量瓶(volumetric flask) 100 ml×2 乳钵(morta)×1 J'\am
, }1 v5 V# ^- G7 `, c50 ml×4 洗耳球(ear wadhing bulb) ^CIi /1 c* F2 T; x, z X! b# X
碘量瓶 (iodin numoe flask;iodineflask) 500 ml×3 T,}mcCyy+
8 T( N3 a/ i; R+ M试剂瓶 (reagent bottle) (无色)×2 889r49{4| / \* L. J1 L* D1 }
(棕色)×2 配洗液: na<6a Z;#G
# k) U( S: [+ Z2 G' {5 F1 j量筒(cylinder) 100 ml×1 K2Cr2O72g+5ml水→65mlH2SO4 _|IM WNB + J1 G0 s6 K( n1 e" x+ V9 a6 @
(graduated cylinder)10ml×1 边加边搅拌(stir)。 ]07B?Q@l ( c2 O# j% h3 j( b+ U" \& `
`(ZRcocqD
% J @6 j3 i. ]! y$ s# J# a6 H8 @二、台面上仪器: 一般仪器的洗涤(wash) /q,_=@|_B / h9 [, J% {- p4 \* x. }, S
铁支架(siderocradle)+蝴蝶架 MvDSY+7y
' w( h! g+ g8 q2 L/ i+ D. j白瓷板(White Porcelain Board ) (一)清点仪器(to count;to make an inventory) cl)D/,$
2 @/ E6 W: e4 B酸式滴定管(Acid burette) 25 ml×1 配洗液 (Lotion) f DGB?z)e
7 ?# Y& O- `- b$ }* N" C: v$ p碱式滴定管(Alkali burette)25 ml×1 一般仪器的洗涤 x&in) ; z# t# m0 k2 Z# u4 J
Y4FxxK" ' @% o/ r2 ~, l5 z2 c
三、公用柜中: (二)滴定管(buret;burette) 9sY/8
3 h$ z- g1 y: g& Z+ ] ^. L+ t直型冷凝器(rectocondensor)×1 容量瓶(volumetric flask) 3H)Qe{/7 1 ~; J. X: J' W6 ` W6 `$ I
漏斗架 (funnel stand) ×2 移液管(pipe) Ti$Z5+2: ' M' G0 I/ L$ E& [7 R: o' L
水浴锅(water bath kettle) ×1 ++4}k]|]_4 ' M9 p" w" g8 o% c9 @
温度计(Thermometer;hygrometer;hydroscope) ×1 0uZis>YD
. z# c# Z _ i0 G, x0 @/ e电炉(electric furnace;electric hot plate;electric stove) 四人一个 q [s6G'zo
9 E l% i- `/ `1 c+ u( m- oDr5. sRP; ! M7 `( @ J7 s% i' P
《分析化学》上册 Jmz E0'
4 y2 J/ `' y- |) i; ]( ~( _第一章 绪论 PsYlYtf
) Z: T' L" ^! j. N) j7 g分析化学:analytical chemistry '0&w6D]47< ) |6 p7 Q5 G ^
定性分析:qualitative analysis {[_y1=uX
) F5 L9 E7 c( ~6 b# _% @+ w" M% D/ U定量分析:quantitative analysis Lo=!h+.gn
& ?: O+ q' ?7 N; \/ R物理分析:physical analysis 6 "^|f$eX * u1 H+ z% T/ R7 n
物理化学分析:physico-chemical analysis 1!^RP&
/ `3 e) D6 D9 U, v8 z* `! o5 V: @仪器分析法:instrumental analysis H/Bfw^[F
+ ~0 F* z( J" O% J3 U, ?. p流动注射分析法:flow injection analysis;FIA ^#N P|Iq Z. l9 Y0 n( M* C' |
顺序注射分析法:sequentical injection analysis;SIA |u6{A $[X
% M J% m$ @# ?4 x! B& D1 w. k2 _4 c化学计量学:chemometrics ? B9(\3h"2 9 m( S8 w7 ]$ G0 s
,C=)xZ ) T% Q3 C* `7 U3 x o9 P0 e
第二章 误差的分析数据处理 1L W!ek$f
1 s( {, o6 q9 c6 P6 R. j! @绝对误差:absolute error 57#JqjkA + q- j+ ?" ]2 l4 }) [! v" Q$ Z
相对误差:relative error /MF:h H]
6 `2 q4 h- O1 T3 E系统误差:systematic error ?yV[w
& U3 M- I Z2 R可定误差:determinate error SXd }
, g3 W- h( O& O随机误差:accidental error rAwW >*
" u/ C% O4 |) q' r" I$ V# w* O% A不可定误差:indeterminate error u@Wa-Te % L1 Z* R/ P3 h2 I# V
准确度:accuracy cG] X214q 7 V2 V6 X7 V7 `; _
精确度:precision FN= co1 ^
. ], Z0 ^. N* h) y7 Q$ u偏差:debiation,d U ~Ln>f
- {# \% M# H8 p- V平均偏差:average debiation a?+ME: + \$ t2 }: b4 A" S& T
相对平均偏差:relative average debiation O %&r*OnW & i" p c. p# e" S, b
标准偏差(标准差):standerd deviation;S :%wfYl?4
# N0 g* L( T9 m0 n* M& e相对平均偏差:relatibe standard deviation;RSD 0! ^\(7, ; Q" {7 w; _) N7 m) s ]
变异系数:coefficient of variation wP{vJe
+ W Q# z, X. y2 d误差传递:propagation of error iRn^)aq !R
8 e$ k3 K7 }3 q# N0 v4 D有效数字:significant figure 1 :ygAe-r 6 B& K& y) @7 m, i& ?
置信水平:confidence level T+fUl 2 ?: Q7 }& O: }3 S" e" B
显著性水平:level of significance HYa3Mc=w , i; o+ D! j! Q. `8 w
合并标准偏差(组合标准差):pooled standard debiation {ezEgA|Kc5 * l$ k: U. w2 c% @ B! j( m
舍弃商:rejection quotient ;Q jNaw0<~\y . O8 F: B+ r4 G/ i5 T
u]nIXWTB@
3 ^- x5 a% e% W- N2 |化学定量分析 &"boQpHr
1 p, ?- D: s: ~; _第三章 滴定分析概论 a1i)u{ a 6 ]9 X, z9 R, w. v; x6 ~0 n& @" b
滴定分析法:titrametric analysis Ykh )P
+ e3 A% U3 E0 ~: A* c" D3 w" A滴定:titration Kk"Z;~DCU
4 V v& f6 E Z {$ z容量分析法:volumetric analysis rc +z/n1
0 s- O2 ?" y& i6 O, K化学计量点:stoichiometric point a4GAnz-RO
/ W# Z+ {7 N0 z+ `. N0 G6 v等当点:equivalent point KStb:
4 s' ~; V {: f电荷平衡:charge balance o<X'yY/y # C8 @* R; V( l1 I; j. M( E. r
电荷平衡式:charge balance equation T-\5G[Z{
) w( Q9 ]8 d4 I: K+ }+ ^, b1 W质量平衡:mass balance N%iiog4
/ b; @4 A/ x# f+ p: {0 `物料平衡:material balance knht1'x:# , Y% S9 P. L* y# J. d
质量平衡式:mass balance equation EYdToo
' b: @9 G) f/ }, U2 ^+ S' R) EyW +u9=e6
+ Y1 F, f0 y' |2 h& n第四章 酸碱滴定法 TmJYSc 8 B7 ^" N" i' u
酸碱滴定法:acid-base titrations j,RKj
* l# H& V0 N( R+ y: f Y质子自递反应:autoprotolysis reaction .2 yV!e}P " u" r% r- |' e! f
质子自递常数:autoprotolysis constant @{Q<=,H` 1 K# v5 ^$ b4 X# S8 M7 a c9 W& t
质子条件式:proton balance equation YXrxTKK_MF
+ m+ Q; M3 E+ U. U w酸碱指示剂:acid-base indicator %~lQgL*o 7 a- S) i/ a* i* J L
指示剂常数:indicator constant *ha n
2 E6 ~ t; g3 X- p7 I" S7 b变色范围:colour change interval 6 }]~1uOo
- e) @+ o( A9 O+ U, R4 x混合指示剂:mixed indicator @w$s"3@,V % d: k3 \2 O6 s; r9 ]0 @4 q
双指示剂滴定法:double indicator titration jX.z
* e% `$ m& |- {2 D# `6LxG.J E # B' I3 F7 m7 m) H( w! g, o
第五章 非水滴定法 h7@7Kr[a % y$ W. n" D. n, x, _9 _5 f3 D' r
非水滴定法:nonaqueous titrations "EY->%yp*
/ J4 U( q' L l. Y质子溶剂:protonic solvent |uB]h/Io
5 S+ b* i. q, a8 [8 i酸性溶剂:acid solvent ;KzqpzzWv 3 ]2 a( \7 [ o* X6 A- O
碱性溶剂:basic solvent #ed.N9!~d : _) b. x2 l: k
两性溶剂:amphototeric solvent V FP-dl
: ~. b1 o: V5 G. ^& V无质子溶剂:aprotic solvent R-CW} Q#~W
# J- [5 [; _% u# z5 ?& G均化效应:differentiating effect 4b(S^<,hg' * G: H5 B- Q. i9 t7 O5 Z3 \1 d( @
区分性溶剂:differentiating solvent 0W?M/n 0 J. ^8 b, g2 m0 C. I
离子化:ionization 'MN~5+Ja
* ^% z9 f, {" m8 O) a离解:dissociation ijfO}2a7 + T+ A. _" L2 W1 ^0 t9 _$ r1 w
结晶紫:crystal violet }]!(6w8n* 8 J+ ~7 ]0 F8 ^9 X, X
萘酚苯甲醇: α-naphthalphenol benzyl alcohol 3>pi)Y sB
* S+ ?% m% r# d0 r3 b9 u/ @/ F奎哪啶红:quinadinered \t xOv ~, 0 E: O8 k0 O( ]0 k. d/ W R
百里酚蓝:thymol blue ~|*n'>{0
/ b* e! |) M! O( Q8 p偶氮紫:azo violet Wl&s>b ! S) B( B$ o% I& V5 X
溴酚蓝:bromophenol blue vU(WnsRD
1 c' j* ~& s, C k: W. J, ~8'(,[y
* L5 k* y& K; M7 ~第六章 配位滴定法 lR73 R|; 3 U6 @" ~" l" a% y" o0 ^
配位滴定法:compleximetry 92Aa)"`
7 L: r; A& E/ L3 H1 ^乙二胺四乙酸:ethylenediamine tetraacetic acid,EDTA 0{+gG^ 0 c, N/ `* f3 F i6 n
螯合物:chelate compound Q2NUq<`U 4 d0 ~# v$ M1 B/ ?2 I4 u9 y
金属指示剂:metal lochrome indcator }7!=@Zb)m|
" A1 c0 [( s$ @<C,p sMD8
9 X# r/ G( K( H: b& t$ ^第七章 氧化还原滴定法 .as ] r N6 ~8 h* ]2 k, B& Z
氧化还原滴定法:oxidation-reduction titration id,]74gBqx
* s6 K) C# {. w, N1 h碘量法:iodimetry e43uWyY . v5 L$ T) `5 _) r5 c7 L0 T
溴量法:bromimetry ] xfx\`@B s 2 ~% m& _ r1 B% ]$ l. O: N, {% g
溴量法:bromine method W _E $ki
; ~" K8 Y3 P, N铈量法:cerimetry Ki~Y0Mu
( q) j h I# ~) m9 q" x" z高锰酸钾法:potassium permanganate method &R~Nb'(t " Q$ Y) f- W% ~* S( ?7 D5 \1 |
条件电位:conditional potential x}dvt{=N{ , Y5 m' |9 t* G3 v& n: Z
溴酸钾法:potassium bromate method y}ec=u
3 e$ ^. K Z( T& ]硫酸铈法:cerium sulphate method !$40-];|^
3 f4 d8 v% z2 k2 ?偏高碘酸:metaperiodic acid o8<4i(qQ`
1 Z5 f5 X/ E6 d) f( @高碘酸盐:periodate ]LZ)ZG~
, P/ N, i6 p! z: v亚硝酸钠法:sodium nitrite method x X:\E-L , I0 j" T" b7 Q; X C( f2 d& X' v' @1 x
重氮化反应:diazotization reaction ~ F?*cWw / T- T4 a6 E; h k( A$ `' c
重氮化滴定法:diazotization titration K5v3YJt-#}
A2 a+ y8 Z" ?/ D( \. _亚硝基化反应:nitrozation reaction AMDk-y ! x# C0 x- }6 e- p
亚硝基化滴定法:nitrozation titration *<~nv647 % Q+ O+ C/ x s8 y( l7 v
外指示剂:external indicator SyV]I A ) ?$ T7 y- `7 F" h, f+ k# W2 m
外指示剂:outside indicator PA'2a RZ
5 m. p1 F( n" O1 ^重铬酸钾法:potassium dichromate method F0|Sla"2^s
4 h( Y4 S. `* @) x/ g L& T2 |+ x7 WFW\V(BG 6 t2 b) E) s" n' e# C7 e9 y- K6 \
第八章 沉淀滴定法 \&&-pMm)
" u) P# W! }. A$ h. d沉淀滴定法:precipitation titration 8G0@<lJ0 3 L% \$ `( U" b' d" `6 N( |9 a
容量滴定法:volumetric precipitation method $R!| 9
* d' q! E! D5 ~+ c5 S; |# ]银量法:argentometric method aj Jjgs;
4 x& T6 y! r8 d( Z! fa$ Bt;tm
+ K1 Z/ Q" w9 G0 Y" H5 M, T5 w0 ~第九章 重量分析法 Gmn7u2>?} & O$ `, P0 E- b6 g( x F+ @/ B4 b
重量分析法:gravimetric analysis w6DMAH>&,*
5 u. s5 q+ f% U: {: X& Y2 W挥发法:volatilization method &?Y8%8m 3 ^1 _8 J# H" J1 w T" F5 n
引湿水(湿存水):water of hydroscopicity k)}XI+T?
( e& R, o# t) H% s ?) B9 I包埋(藏)水:occluded water px[(?j6!R
% T2 N X, Z$ F. \5 L吸入水:water of imbibition &csor;0cF 7 V2 l! u1 e1 _7 E9 R6 G1 S) R0 t
结晶水:water of crystallization x\s 4W>y, : b: M' I+ C6 u$ Q; Y
组成水:water of composition 7wrmVaB
. d8 I0 d0 q% B' E% t' ^液-液萃取法:liquid-liquid extration ><N(B.?e / L5 I9 J* V6 ?- U7 ~; R; \
溶剂萃取法:solvent extration \Rw/^*L6l
4 p9 O: v9 C) u/ @* T; F反萃取:counter extraction @l&%X_7( ; y! T0 V! b0 A
分配系数:partition coefficient QO} y_~@
/ V( S5 u; x( X; t分配比:distribution ratio ElI^z 9 N9 a, f) E O& d3 y- ~7 L! M3 n
离子对(离子缔合物):ion pair 0E)jX>`F W" c3 } b! Z$ Z: C9 C4 h$ ~, F
沉淀形式:precipitation forms '3wIN!c1A
6 n% ?" [; f4 u& b称量形式:weighing forms aLgzzQS
1 g7 \4 n/ p3 q/ A7 m) X. k4 g ?(58 ~^K5
1 O7 O; f0 }7 c《分析化学》下册 m@.0up?3& , ` P& w V& v/ w
仪器分析 概述 on@pn[`aL 4 Z% N# U( P" w5 H
物理分析:physical analysis :E4+W<otBn
! _* o1 G' C& K物理化学分析:physicochemical analysis oa6P {G
( X; ?) G( m) _* S6 t$ @9 Z' L仪器分析:instrumental analysis 4Sab}0W1
+ K: l) \" r4 F% h @1 i[e<xb 0 ]: v4 [8 Y1 m7 o, s8 E. s! V
第十章 电位法及永停滴定法 :\ "mv 5 Y& N* T; B2 B: L8 S9 Q" g1 _
电化学分析:electrochemical analysis "~^ [ P \: l$ G4 ~& F/ j
电解法:electrolytic analysis method ax=#QCngo8 $ K D1 q/ m+ m' H
电重量法:electtogravimetry v=2tlwY
/ \( Q! B' t! x: d库仑法:coulometry :Fu6b&uq<
7 P# {, v* Z6 h7 u q6 o, [% S库仑滴定法:coulometric titration Ngyv4CF+a , ?* v, {" r7 e
电导法:conductometry Pil=(%s - r u6 S0 I/ G
电导分析法:conductometric analysis H9}q!1REa 1 b8 i, s! @# m
电导滴定法:conductometric titration yR?p#+8
9 ]" I4 p3 |: Y+ f; u电位法:potentiometry |tZnJ3`X
& h# \" L& ?6 q/ N( a! g3 {0 y; o# D直接电位法:dirext potentiometry .a6@?8-(z * V5 O1 y! f0 k* @! N6 F7 U
电位滴定法:potentiometric titration T/Nn^hq7 0 E5 E9 {. \ [, F+ K. j
伏安法:voltammetry t#BOm 4[ % c# M/ }. f& V
极谱法:polarography Xl)..<4u,
% w1 U3 g$ k" |' _溶出法:stripping method u9Q/[7*B}E # Y3 o5 D3 I. b% k t7 X, G- D
电流滴定法:amperometric titration nmcw7R
3 G) j& Q. }/ ?化学双电层:chemical double layer IxlH .
" I- v, H; Z0 _ {* Q) B$ k- j* U相界电位:phase boundary potential 7!]0?DfM6
9 I0 k1 t. O! |. ?: c: j金属电极电位:electrode potential 1ke3);p
@% l* Z3 `- _# P5 R2 @$ m化学电池:chemical cell .byxJ6eD@o + D5 O' u' @' [4 e% @
液接界面:liquid junction boundary !h 7`cRz 5 W: f& g6 k7 X& }
原电池:galvanic cell 4Ey_4n
+ v/ Z0 E& R5 l9 L; w( A, Y电解池:electrolytic cell JrH2TQu:
: O m- l. g: ], ]负极:cathrode q,< 4 1 G* M$ t# ]+ G* n
正极:anode <\Z'g?~5
* c5 W2 R5 i! {" i5 O4 @! r: x. Y电池电动势:eletromotive force ,!JB"%S%)$ * f4 q* s& T( ^ }! Z4 p
指示电极:indicator electrode S~y<?wDD#B . y' t: b. X7 Q" v; a; s
参比电极:reference electroade ?|} ork. - }8 i" S0 ^3 w) x: T9 u
标准氢电极:standard hydrogen electrode 0kmWFq / p6 S! g4 |5 s# E4 L4 a% m
一级参比电极:primary reference electrode iW!9oS>
# I0 r" N2 X5 W) F! W饱和甘汞电极:standard calomel electrode x"Mks"f0
+ W5 S' } [+ I$ R银-氯化银电极:silver silver-chloride electrode aN-dEAP 9 F8 A: }. W2 f- E0 m
液接界面:liquid junction boundary ;Fnx&#kH&
& _1 y! N+ E1 d q不对称电位:asymmetry potential Z!xb`k&n 4 t* C9 D% T" T! c5 o
表观PH值:apparent PH B:%x!.k\ 3 p& r; b/ U! ^% `
复合PH电极:combination PH electrode !/vUHh9 + |, M/ {6 x' f; B/ t: C/ u+ M
离子选择电极:ion selective electrode =CFF;K
% n8 p$ [1 {" r) c* t敏感器:sensor /Qt9": ; z: k4 N& }/ Z% ~0 K
晶体电极:crystalline electrodes F&B_3>L
; T! H6 \0 u* k( {均相膜电极:homogeneous membrance electrodes FDWEs2
* m2 @8 T/ h3 \" ^8 w非均相膜电极:heterog eneous membrance electrodes [04^_i
4 m; n- B! H; Z) ?- b% r: n非晶体电极:non- crystalline electrodes =iD Ns-
) M' o3 V8 P- W刚性基质电极:rigid matrix electrode y]qi\nw5\
# X9 W$ H4 t F% I9 D: }+ m流流体载动电极:electrode with a mobile carrier `8-n9:^ 7 K" w6 m/ @. K! s h8 M5 m$ p5 ~
气敏电极:gas sensing electrodes JVp;?hj
V( c0 l2 `" O! S4 {, p酶电极:enzyme electrodes XS1i<ZU 0 ]: V/ N0 y" [$ P& U% J O
金属氧化物半导体场效应晶体管:MOSFET ,t>'6j/ W
8 e/ Y: f7 M7 N ^( y离子选择场效应管:ISFET gry\A#1 M
8 G0 t" ~( i. t8 N总离子强度调节缓冲剂:total ion strength adjustment buffer,TISAB #yEb1Df}b
0 v0 ?6 g* s" a+ j3 s8 I! I永停滴定法:dead-stop titration ;ybj F]
+ b+ R t; r9 o双电流滴定法(双安培滴定法):double amperometric titration ?bV{wx]!^ 8 t5 b5 n5 z2 D2 K
+q7jUPE0. # e+ Y7 m0 P+ {$ s% T
第十一章 光谱分析法概论 q&eI,FWV,
$ R0 o- q$ H% l% b1 a( s& P普朗克常数:Plank constant <[-s7#yD
% `% z% w9 K# ^2 U$ |3 F( V3 Y电磁波谱:electromagnetic spectrum )A98=tw $ m6 ^: J3 g, M! V2 J. e2 r
光谱:spectrum CRWT."]L
, x$ Q: Y7 _! ?+ X) U+ ~' p! o光谱分析法:spectroscopic analysis pW%q+?V` * W1 _; {; B3 C
原子发射光谱法:atomic emission spectroscopy jZ0&?&Yr 9 |6 ^3 w5 W0 m2 U4 r* _; d
质量谱:mass spectrum >.^j/~l W
' G9 Y- \8 T, B5 g质谱法:mass spectroscopy,MS EAZ8A9Gr
+ ?1 i% S, v6 k/ W" S# u N9 s: QC_$=|/{O` $ ^. X5 q6 y$ G) x( b- O
第十二章 紫外-可见分光光度法 N Ap /_z 5 N/ N$ f$ y# A$ S8 t% y- ?" V
紫外-可见分光光度法:ultraviolet and visible spectrophotometry;UV-vis o lko k) : c. |; u' h; u7 X" ?
肩峰:shoulder peak #@ ag=}bN
6 ~% \! d: O% ~+ s6 {末端吸收:end absorbtion B yRk !
* s; m @2 J4 t% g生色团:chromophore r5^M9X&k
) i/ f) `) ^; N* F" c3 k助色团:auxochrome h7BFh-G= : N( ?0 i7 c' m+ Z4 L- c- l% @
红移:red shift yY1F8N
8 |6 d4 `- K: P长移:bathochromic shift cv=j6w,
( \ X# h9 K4 d% L9 t. }6 u短移:hypsochromic shift :yg"A{b 7
. n8 h5 q7 L+ r蓝(紫)移:blue shift <&9.lo/
$ O9 b$ k9 M$ s2 b z增色效应(浓色效应):hyperchromic effect Aywd`DA 7 T7 c9 }$ r1 E& i( d
减色效应(淡色效应):hypochromic effect %7^8=m5 4 W' r+ e) c- x. E2 J
强带:strong band v7!45#" , @: X1 G( H. M b7 C, J
弱带:weak band s-4Dzy
% U+ m. {. A0 E9 f, {* _吸收带:absorption band z-DDOT4'! $ r7 F& t+ v: Z" N
透光率:transmitance,T w)e g{}-@. 2 B& X/ }4 b2 Y! z
吸光度:absorbance DchFJyq~D
# X) ~6 F: ~! b$ U; l谱带宽度:band width vPw}GZF2<
" ]* p6 e5 I: Y2 }! D) C9 ?$ z. T/ Z杂散光:stray light K1 Q=h,& ( Q8 n# M, E! ? g
噪声:noise =rb / h\* ( S- M( r% z( g3 ~+ n
暗噪声:dark noise /f[Mc1_ s 1 B @/ s0 e H
散粒噪声:signal shot noise k2X|04!P 9 X! F! C0 a1 @; D" |8 x
闪耀光栅:blazed grating o;E_Ua5 ) : _6 P5 g* ]0 j' v: f" l0 A
全息光栅:holographic graaing 'C|`f%-
! G; m; A2 N d光二极管阵列检测器:photodiode array detector f:M^o{v 4 M4 A) v$ c8 ?3 ` ?0 O
偏最小二乘法:partial least squares method ,PLS U\Lxo%U
# v* R4 E1 l" w/ u褶合光谱法:convolution spectrometry L_^Eh3}e
9 @* y$ Q+ w9 m& k% f褶合变换:convolution transform,CT u\6juX#f
5 b5 ~6 a4 f$ m8 y3 T/ Q离散小波变换:wavelet transform,WT \y-A.YCV
- Y! i& o! o0 t: ~' Q* N- p* m, } q多尺度细化分析:multiscale analysis 5`On 2
@+ Y. B8 E- q供电子取代基:electron donating group /5v) ?}tIb
( p9 h t6 l! o7 _: t; d, r吸电子取代基:electron with-drawing group 3)`I 0|0
' z* H9 F8 D8 A第十三章 荧光分析法 jFFMz pu
- `1 q& U+ Z" A, f/ v荧光:fluorescence H4lLpV]8 , ^! e7 G$ Z! G7 {) [8 n
荧光分析法:fluorometry L ;ePzD
# K- I2 o9 w1 `$ kX-射线荧光分析法:X-ray fulorometry `/!\!*gz|N
i6 h# n8 A2 e3 |$ B原子荧光分析法:atomic fluorometry e5=|Yc$ # z( K4 ]9 G) n3 q
分子荧光分析法:molecular fluorometry 'J,-E|Jxs 2 I- Y: B" R8 n3 Q- ~5 p
振动弛豫:vibrational relexation bLCiHq ?
1 ^ ^3 P1 c9 _内转换:internal conversion ]0K BInZ`= & B" K8 o# [+ U: v- c2 m+ t+ W k" |
外转换:external conversion -Ti?Db} - E$ o5 E2 ~' E- j6 C) u
体系间跨越:intersystem crossing /h'3L{Z
8 s+ \+ p m: v激发光谱:excitation spectrum SOS9})> 6 A2 u0 F, z5 I' l! r) |
荧光光谱:fluorescence spectrum &1Y[0R
z4 b; [8 o! ?' Q% M0 C斯托克斯位移:Stokes shift 6X-|RsZw#
, \0 s8 x; F# q荧光寿命:fluorescence life time 5[op )
# }0 A: r0 @& v+ ^4 X3 E x6 w荧光效率:fluorescence efficiency \{_}dyA
0 ?& ~! T- U F, t* `, |/ ~荧光量子产率:fluorescence quantum yield u?bR&.s
# l& c8 }5 A: o1 q" G荧光熄灭法:fluorescence quemching method NErW>n{., 1 Y/ y3 s% U8 w$ {( F* C
散射光:scattering light ^>KKSq~xH
. K8 J2 g( `( Z1 I瑞利光:Reyleith scanttering light TA ^~' p 4 F6 Z1 d0 }# ]' u9 H
拉曼光:Raman scattering light Fv;bXID(~_ : V4 T1 ]9 T6 ^# g
J9Ls9 . 7 B# e' D4 ^2 p* K
第十四章 红外分光光度法 "h9YnFoM~ 7 Z: F+ k- d* Q; r8 N* V& {% [
红外线:infrared ray,IR }`)OtOToN
% y& z0 ^! [9 E4 t/ Q中红外吸收光谱:mid-infrared absorption spectrum,Mid-IR W8&H%+q*
7 w7 y( `! d0 @ e; Z9 ?远红外光谱:Far-IR 4`~>&TQ!!
9 i" M6 M: u1 p4 B8 X! }微波谱:microwave spectrum,MV <tO7[ ; 7 z0 {$ m! z8 \! e7 \5 Q
红外吸收光谱法:infrared spectroscopy uW%%z65"2 - N& N5 _& H5 L( ^; Q
红外分光光度法:infrared spectrophotometry (; m;yd " l& H; W% W, i' S
振动形式:mode of vibration <~h / 4?
! m2 p$ ~$ B0 n- y) k0 E伸缩振动:stretching vibration rve6f&g[ * D9 M$ o9 z' ~% j" Q8 E6 w! _- N
对称伸缩振动:symmetrical stretching vibration 6>m8lqCbv 2 @4 n! u+ I* d7 G+ G! S1 w0 I
不对称伸缩振动:asymmetrical stretching vibration by+hOZ\
5 L, Q: _6 K% s% C# W2 [弯曲振动:bending vibration Ej/ xb'V ' ?0 q) x- D! W3 V: m4 o4 e
变形振动:formation vibration 4kr,y * 1 }5 M% z3 M6 I1 \) B
面内弯曲振动:in-plane bending vibration,β C7.4 &g+o Y- u$ v5 ~" m+ y: e- {8 Z7 A
剪式振动:scissoring vibration,δ 2xAq% O 9 k, M5 N) J/ f }, y& P% F
面内摇摆振动:rocking vibration,ρ /,yy}$?
; W3 W, K2 B' A/ X# D" M* N面外弯曲振动:out-of-plane bending vibration,γ 4r26^>2T / r v9 f# B1 N
面外摇摆振动:wagging vibration,ω BIr+r:X0} ], F* R4 S$ e, c4 V5 [7 B
蜷曲振动:twisting vibration ,τ xJQm|{P(v
U2 |* K5 i/ w E8 M1 d8 u0 g7 R对称变形振动:symmetrical deformation vibration ,δs ,^8n9>s6vL 2 Q( M& i* i, K+ Q* u
不对称变形振动:asymmetrical deformation vibration, δas Tb55hsC
- V& P+ ~7 e! p2 X4 s8 C. q特征吸收峰:charateristic avsorption band [s/I ~i!
1 T9 m! a9 a5 |- C特征频率:characteristic frequency = J DXBA5 ' E8 v7 [9 k+ Z8 `- s) H# o
相关吸收峰:correlation absorption band txbMk_])zH
5 P g5 s. `) }$ k杂化影响:hybridization affect _2|ZUQqy
# l. L4 ~( v$ l0 K4 f环大小效应:ring size effect a?r(cj
) i8 \8 G) ~4 T6 z } b5 r* m& p; s) k吸收峰的强度:intensity of absorption band .CZoPpy D
/ b& h: \( R& _) ^) r环折叠振动:ring prckering vibration iSzB_{& & U$ P8 c4 C; W0 b+ m9 C
第十五章 原子吸收分光光度法 =6< ~`uHkp " J7 _& _1 X1 p8 O; v0 |) Y
原子光谱法:atomic spectroscopy e_f2:!11w - O! c& e, s" X" \2 l. [3 G
原子吸收分光光度法:atomic absorption spectrophotometry,AAS ZM V'Hyn
' @% d! E0 o. f$ a! q2 f6 Z原子发射分光光度法:atomic emmsion spectrophotometry,AES K%7m !?Z 3 I& {4 C5 c2 i: l
原子荧光分光光度法:atomic fluorescence spectrophotometry,AFS s? -lS*)P
" ]5 t) W# C4 u1 w9 p! I& GG,0:E.~5}
* G! ?1 M3 n( o5 w" L8 I第十六章 核磁共振波谱法 H>4{Y-7lM9
5 N d0 F% t1 ?% T% t核磁共振:nuclear magnetic resonance,NMR r`\tPQI 8 j U' m& K4 l; J7 D; C
核磁共振波谱:NMR spectrum GO3&>1*{~ X4 p" o: F' O" V
核磁共振波谱法:NMR spectroscopy Cs=taPq 0L
: O$ S( J3 t" ]扫场:swept field MgoKH5 . v9 d# i" ]+ N# ] W& W* b! W
扫频:seept frequency 7=9( ]n
) ]% l; [6 N% f5 X/ x连续波核磁共振:continuous wave NMR,CW NMR N4m9L'"\ - X0 P$ [* {- J% ~; S
Fourier变换NMR:PFT-NMR,FT-NMR 98YJ
C2 l6 _0 X; {% a3 ^- e8 I二维核磁共振谱:2D-NMR [G:2!r50ap 8 L% `4 x) Y& w2 X5 @* I
质子核磁共振谱:proton magnetic resonance spectrum,PMR B>vfQ=f;n " T1 W8 M& {) k& `
氢谱:1H-NMR @U*N<W+0;
. A9 t# L8 M/ Y碳-13核磁共振谱:13C-NMR spectrum,13CNMR X_ p<.e 2 M P+ O& @0 p% X8 } k# Y0 J
自旋角动量:spin angular momentum Z K3~d:p
/ s" P6 n& `/ y磁旋比:magnetogyric ratio 6ILA2, ' m) l6 }1 U' C' S) U; x7 E
磁量子数:magnetic quantum number,m 4'1lIZW
7 I+ s5 Y% ?: r# T8 u进动:precession 8ORB#&{6 5 a7 C6 Y' D. K4 U
弛豫历程:relaxation mechanism &;xe% -s/S 4 ? [3 G5 H0 F
局部抗磁屏蔽:local diamagnetic shielding Wz&_kHu
2 f+ @6 j) e5 L! S9 K" Z, a屏蔽常数:shielding constant 1}}:BwDGf
9 s: k0 f* q2 e, M; W( P: H& ^& \8 c6 I化学位移:chemical shift 3P!|3hj
6 [; j5 R& D+ o7 p2 y国际纯粹与应用化学协会:IUPAC H;;r6^@MM 8 b. N3 a4 h! r2 m: E
磁各向异性:magnetic anisotropy )q & ~ 0 U( ^' V1 }! [* i# b$ j: { o2 t
远程屏蔽效应:long range shielding effect 6: CsR 7 F( Z. I; Q6 G5 M; y; x/ r3 b
结面:nodal plane jqx%Sp8, 3 E# |& t" d! z7 ~3 Q% n+ Y( |
自旋-自旋偶合:spin-spin coupling 1 O%t9x / ?+ f3 U: n" ?2 d8 X% v
自旋-自旋分裂:spin=spin splitting '2+Y~\4 oT
5 J6 @& G$ Q) n6 o! l单峰:singlet,s f1} '%rp
& e) ~- X3 F0 ?. x双峰:doublet,d BTwr ;K
2 i- Y* h$ j8 o三重峰:triplet,t Qlfxq ThA;
3 k6 t" s8 F% @ l四重峰:quartet xo}u s31'N 6 k2 z1 S. k: U+ q8 g; j
五重峰:quintet DO d6N"
7 ~9 D& i% c+ r$ D( r六重峰:***tet AnZx i e
2 x# C1 l1 x. T$ {偕偶:geminal coupling H[8nq{0 @ " T/ l% M1 j3 C% A1 n
邻偶:vicinal coupling t7:M+Zy
2 k% f! b$ T. ^6 l& A) V0 V远程偶合:long range coupling $S+N1, . \: E% E! l- s B1 V
磁等价:magnetic eqivalence /l;x \tk% $ ^/ ]9 M6 j$ L7 M$ p
自旋系统:spin system bUVsN^%A
3 o3 c8 {. j! v+ T一级光谱:first order spectrum +-(riFEX@
, U- b7 L' {$ _! P二级光谱(二级图谱):second order spectrum RbuWhD!& / U8 U E$ o9 k1 l8 A1 _
C-H光谱:C-H correlated spectroscopy,C-H COSY oFHvTf6V
4 V& H% {9 P- k% m5 |3 M! I* h0 Z: L5 b# S第十七章 质谱法 Z9~(WcBz
. ^; X) Z% B: z2 p3 g质谱分析法:mass spectrometry wwZ TFJIjm
* u* I1 j) I- f6 j! j5 u( {质谱:mass spectrum,MS ayPb(Y4
- d+ P: ?& L* m# ]! C |- v3 n1 }' n棒图:bar graph # @ PhRFN
& L; N3 y6 l- p% S选择离子检测:selected ion monitoring ,SIM %-="NoumzO
, i5 P1 Q) o5 U, y7 c直接进样:direct probe inlet ,DPI L.eDC&xFt=
3 D2 n3 A0 F; W6 h6 M) n接口:interface daQ6_,\w ( h5 O0 z1 E, i9 M- W9 S
气相色谱-质谱联用:gas chromatography-mass spectrometry,GC-MS 4?BG&J5Q{ - ?9 _1 Q; _1 E, s& Q
高效液相色谱-质谱联用:high performance liquid chromatography-mass spectrometry,HPLC-MS zWUXx29 W
- t1 q, j2 F8 V. ]( r Q9 g) Z5 E电子轰击离子源:electron impact source,EI vjUC,aO6X 7 H8 G$ n( F' ~
离子峰:quasi-molecular ions 91[w,$n, ) l# _ A: v" q1 H
化学离子源:chemical ionization source,CI c1dp/@
7 h/ K% n0 n. x B0 b! A场电离:field ionization,FI z!c@31D
; h- H* R G" H0 U场解析:field desorptiion,FD Cf VC^O\G
% y, R M+ Z4 l快速原子轰击离子源:fast stom bombardment ,FAB =:U_8(K ( }0 O+ C* k* Y4 |* r. D6 i
质量分析器:mass analyzer .q)) T
+ J2 u% u3 A/ l4 \1 b磁质谱仪:magnetic-sector mass spectrometer q&V9/rr5#
0 u6 ^& [2 \+ G. v. A四极杆质谱仪(四极质谱仪):quadrupole mass spectrometer @DLdH
" N E% T- }/ k8 h4 e" p- o原子质量单位:amu K8:xJQ(A}
6 k, o" j y) S; x离子丰度:ion abundance q?$X+;\
1 C- f" m/ Q/ o/ f相对丰度(相对强度):relative avundance J_ZFZJ cP 6 C3 w( |% x- @/ e2 @" D
基峰:base peak 'fA3{P-: ; B3 G I1 ~1 u/ s2 T8 U! T1 W
质量范围:mass range PZhj i}
/ L7 D5 C( p. x6 _ B8 l6 g Q分辨率:resolution >k G$* 3 N& {# H5 h! A
灵敏度:sensitivity 6mEBzR#*
/ p7 V' u# c; A信噪比:S/N qF!a4 j
+ V7 {, T7 e6 M0 D分子离子:molecular ion ln6a| Gc< % L: J/ P5 M% R, A) G
碎片离子:fragment ion ,kD&6r7
4 F" b3 e7 f+ h U; i3 `# ]同位素离子:isotopic ion Q7Px.Gb8Y
- Q. g, H6 I; @1 E. H/ B* m4 G亚稳离子:metastable ion n"G.Pf^ 9 d0 i7 _3 ^8 m q
亚稳峰:metastable peak %{63| '{ 0 C9 ]5 u2 e( E3 R3 l8 ~
母离子:paren ion L=ZP_8n$
8 g% @- \ k. E. Z% e子离子:daughter NSox Dre|
! Z9 x+ u$ G/ Z含奇数个电子的离子:odd electron _BGw74!.cy
; Q' R/ ~% H% E4 H F含偶数个电子的离子:even eletron,EE x r?PD9 + X2 @2 y4 z7 o+ w9 \
均裂:homolytic cleavage ru'uuRX~ / g2 @0 z3 K0 b
异裂(非均裂):heterolytic cleavage IeiWrs]X $ z4 j. m. Q0 d
半均裂:hemi-homolysis cleavage ([xXy,Xh $ y( r, y! L/ x; ?' b6 l7 a4 _
重排:rearragement WwOT}4_
$ D* [/ Y9 p& S' h分子量:MW _fqU(G?d . r( r1 r7 D+ G% N: _
α-裂解:α-cleavage e$Q+n_o
6 x* @1 S& z5 Q3 ~5 ?" ?yq\OFme% 5 w' h- d6 n' o* O
第十八章 色谱分析法概论 1:Kw=s^`S
% S. i" h2 i4 R" j6 f6 `. o2 \色谱法(层析法):chromatography o0kQa _
& o6 O. o+ A$ o固定相:stationary phase LTM4`e}q! ! z d6 {" E9 o. G# e8 N' h% h
流动相:mobile phase Q&gX` 282
" E: l; E7 }3 K超临界流体色谱法:SFC 2? Em )z9
U$ m8 I5 H+ n+ c' C/ r高效毛细管电泳法:high performance capillary electroporesis,HPEC * qG _H*
, i! E5 K* C% y7 E气相色谱法:gas chromatography,GC 6n8 \~x${ 6 S+ I! {1 W ~" t& J
液相色谱法:liquid cromatography,LC Dz 8w=
# f6 m1 |8 [& y超临界流体色谱法:supercritical fluid chromatography,SFC )21J"%R
O$ E0 k2 w# }* ^- s气-固色谱法:GSC ^md6*H"<=<
9 ~+ U* z$ \- i0 Z) b6 ^# g( P气-液色谱法:GLC /k 7 6 o' x7 [* q/ t5 B4 S
液-固色谱法:LSC yo\j " b" U. k' ^8 X$ N v! N. W+ h/ l
液-液色谱法:LLC L o\wp\[ 2 p L V J7 M6 O) @$ @
柱色谱法:column chromatography y"_ccw-L 7 s1 z" Y5 b7 \/ h# F
填充柱:packed column -zh* V 4 R( d3 L$ u8 Y1 o
毛细管柱:capillary column ,"Q}s;d ; P$ Z4 i$ @& w3 _& l2 L( v) Z3 ^
微填充柱:icrobore packed column P^+N]yVn'
( `" o4 j, z5 [/ G, A高效液相色谱法:high performance liquid chromatography,HPLC Vb6 !YzVPA
3 ?" Q6 c7 S* h1 H- V平板色谱法:planar VFT So 1
+ Q: }7 `5 U+ D" |* c2 H平板色谱法:plane chromatography V=E8HC % ^, R1 a5 ~" y% c; W* |' P7 {
纸色谱法:paper chromatography [-s8 Uui9' M7 B% y; V9 w$ a; M
薄层色谱法:thin layer chromatography,TLC >0,y v|
/ L9 t) m9 N$ J2 u- N薄膜色谱法;thiin film chomatography M9~) ;N2{ . v# t# u; Q! d1 q) r5 q
毛细管电泳法:capillary electrophoresis,CE _E %zwm=
% Z7 {" E6 T& `. v6 x分配色谱法:partition chromatography jZXfe3 $ }/ o _. v0 U& s+ ?. h0 `6 P9 Y4 E
吸附色谱法:adsorpion chromaography +#8Z;m$(* 7 @$ \$ j' [" m$ f Y
离子交换色谱法:ion exchange chromatography,IEC SVg8C4
* C8 Q. k3 L7 M空间排阻色谱法:steric exclusion chromatography,SEC G$I 4PPrI?
2 `( d5 R; o' f2 c0 K亲和色谱法:affinity chromatography -tWRB?/}^
% O% D9 \- [+ Y$ D, r4 X: v分配系数:distribution cofficient IT (=-r$A: 5 j, X9 Y4 j2 k, a
狭义分配系数:partition coefficient P$EHW7,G : v! @8 z2 J6 `, O8 x/ s
凝胶色谱法:gel chromatography )%#Tq|wI / O/ w& H! C* z# `) o. e
凝胶渗透色谱法:gel permeation chromatography,GPC )t[WG6 : a% M& }8 s* U
凝胶过滤色谱法:gel filtration chromatography,GFC Ot }/
7 t* R8 j% |9 \7 z+ s+ ]6 @# E6 ^渗透系数:permeation coefficien;Kp 2(<-e
" O* |( q7 W9 C2 t' a$ P化学键合相色谱法:chemically bonded-phase chromatography ^"/(K!7 & Z( g8 o! t' x5 |0 }$ `
分配系数:distribution coefficient eAINRKi
6 r/ O2 {& f3 E! V: c靛菁绿:indocyanine )pZGF&b$& 9 h' `4 w9 A% M( s; B
气相色谱-傅立叶变换红外光谱:GC-FTIR ~k\f8*6*d
9 Q" g- ^1 |6 p- `. i0 Ga4 "@r$
* A* S9 j t+ P. Q) y; O% c第十九章 经典液相色谱法 EHq:+
4 t. A9 I* \1 N5 n% G, I6 B6 P薄层色谱法:TLC laz]F&U? + V. c$ Q7 ]1 p. u/ s6 K
吸附:adsorption +(M-SG- ( k& L! m3 U7 x: S, T1 ^! b
活化:activation -fI^*/ 5 j5 P$ T" q/ D3 k7 e p% t2 ~
脱活性:deactivation ULnU]D7
: {. Q4 {8 {& Z: j+ Q: I: m+ X! _# n交联度:degree of cross linking t"@Z"7CX
- { `* f; q0 j) C4 `; S/ A交换容量:exchange capacity "-SII3,
' h& ?/ i/ F) R0 O2 [* f$ G' P薄层板:thin layer plate 5Pn [f>5
7 A! @: j4 T) j4 ]展开剂:developing solvent ,developer *hzg<duk . j O5 L2 S( o( j. R+ e0 J
临界胶束浓度:criticak micolle concentration ,CMC z*Kb(3&, 3 L/ U0 X4 }" ~3 c/ o
相对比移值:relative Rf, Rr )4|^=vpD 1 f S* X! Q+ T0 F$ _
分离度:resolution ,R V&xNMC]f0
4 V l5 A: G8 d2 q: g分离数:separation number,SN ;\}*r9)V
, e& ?$ c, K* ~ K9 U. W# L+ W+ o煅石膏:Gypsum 6Ja,X^g`<- O5 U- {1 R7 f% Y i
羧甲基纤维素钠:CMC-Na DoyLEpmb1
2 d7 y3 w, Z* X# K4 R6 }5 m吸收光谱联用:TLC-UV yz2k wZx
; J6 u( p2 `+ O* @+ ?. s }薄层色谱-荧光联用:TLC-F t~9W98 0 I# B( A; S0 x" i; F, w
薄层色谱-红外吸收光谱联用:TLC-IR Vy)Ks6:~
^6 q& U' Q3 q, ^, G$ G+ U$ i薄层色谱法:TLC-MS yVt@ZwMu % m/ B% W2 Z! Z7 |- t
纸色谱法:paper chromatography *Z$)>WRZ!
2 ^: }+ E- \6 G( C) O上行展开:ascending development [bTLx,Ue 6 @/ u7 y$ ]. {' G( @' V
下行法展开:descending development FrB>ihz
$ g. r9 N, ~9 T7 h2 ]) g双向展开:two dimensional develoooment sr5pRc`\
8 Q/ o0 t5 g; s# S1 _' Y# i|2}yN3M)>
/ v; g% O9 m, W, _8 ?- q; {" H第二十章 气相色谱法 m~^&~ . r! k( s+ g6 ?/ m r4 c/ D& R& j
气相色谱法:gas chromatography 4 $cX[ * P) a6 a6 M+ ^0 Y" Y- f! E; [
前延峰:leading peak [51Q=.~'
6 g6 G$ o i% J. C4 b5 g/ H拖尾峰:tailing peak M9xph> X
- D8 |* m3 ~* z0 n k4 z对称因子:symmetry factor,fs C,v<mu'g !
( N4 p( A9 T+ y" O4 g3 y0 N: [. ^保留时间:retention time (";tU k$j
; _) ]; ~. y; }保留体积:retention volume uu]{N: wA ! ?7 [" w8 X/ g
死时间:dead time m](rDy" ( t |/ |5 ~ g8 @+ m
调整保留时间:asjusted retention time \lpI&V^3 + u9 g9 O$ c/ w+ g" X/ F
半峰宽:peak width at half height,W1/2 or Y1/2 i~-QK3r~
' _2 a+ w5 q/ F' C峰宽:peak width,W <&]N` YZN : |5 ?7 K( A$ _- p0 u
等温线:isotherm #LJ 2Q
2 ~' f ]# H" w: y4 n理论塔板高度:height equivalent to atheoretical plate |]O 7 .Ngb . w- n1 X) r9 b9 t; O9 s5 F
化学键合相:chemically bonded phase xJXe*.b'S 7 l" h* W$ I1 t; _
丁二酸二乙二醇聚酯:polydiethylene glycol succinate,PDEGS,DEGS Tdd/8JF 7 e9 } |8 y4 v2 @$ Z
高分子多孔微球:GDX gi^DwLJ_ ) w2 a. c" F2 c( A9 g
苯乙烯:STY h uN%;-x 6 D. U( L* \ C1 f' H( }; {
乙基乙烯苯:EST cGcK>1i ) G; |: j5 }$ y1 c! t/ ^, l
二乙烯苯:DVB V t&L?es
9 a& r5 J. |0 p& }涂壁毛细管柱:wall coated open tubular column,WCOT }M*bPm0
+ u/ w0 ~& B- q. r O; s载体涂层毛细管柱:supprot coated open tubular column,SCOT `yr4)x y : b9 c0 s7 F6 b* U/ [3 h& I( A
热导检测器:thermal conductivity detector,TCD pB` iSL[
1 q5 P: M! j2 r8 H8 w' \氢焰离子化检测器:hydrogen flame ionization detector,FID x?qAvu<Idk 8 F) m, ]! g# y. y% Z& J: _2 x7 t
电子捕获检测器:electron capture detector ,ECD 8XWJ}o 9 {" x3 w6 ?: }( }$ M- |
噪声:noise,N 2I*V?XXQk " G; j, f- {1 x5 Y( }+ i
漂移:drift,d w}t<UQ)l
8 G! G- b( {6 u8 O% Y' P灵敏度:sensitivity 75Z$S.( : p9 }5 S. ]# b1 C5 s) x
检测限(敏感度):detectability,D,M (Zd^ \ - w8 a5 d6 V; e" n2 L$ v; r% M
分离度:resolution C.>4&dMW
0 R) A8 w, d. p) A& l& d7 e归一化法:normalization method T v,c'b
E p* Q+ Z! U) P L; {外标法:external standardization ^l.{S%|4
2 J2 ?5 n, }; Y=@V<[%_ + J- j5 |; s6 G: f
第二十一章 高效液相色谱法 R+)=DuYf D ; e& W: T+ j$ ~4 H; L5 x0 j, K
高效液相色谱法:high performance liquid chromatography,HPLC YUL<?pO I& T& t2 p4 L9 ?
高速液相色谱法:high speed LC,HSLC +~,~x*P4N%
$ Z1 K. L7 }" z1 K/ l高压液相色谱法:high pressure LC,HPLC K[ntjHTqE
5 m6 B9 i# {9 j; b$ g高分辨液相色谱法:high resolution LC,HRLC znJ&"p8: $ [6 E, E. E1 b7 I. v
液固吸附色谱法(液固色谱法):liquid-solid adsorption chromatography,LSC Z,P5q$ + A' O6 U7 o; F$ S9 x8 _, \; V( F7 h
液液色谱法:liquid-liquid chromatography,LLC ()b*Sn> : G7 E {; Z8 a4 o, l4 B5 J$ K) \
正相:normal phase,NP agc^B{G(
$ E/ k) C H9 I) w8 ~5 d反相:reversed phase,RP Nd.y] y/
, b" t9 H! H8 R' c化学键合相色谱法:bonded phase chromatography,BPC GZ}42R/gC ! Y9 J D4 w! U F' b. p- ^
十八烷基:octadecylselyl,ODS fM=*vE)h!
& ]7 J9 i7 J+ h5 Q离子对色谱法:paired ion chromatography,PIC u1L|NGEY 0 K2 |4 x% T' [
反相离子对色谱法:RPIC <]! H 1 T$ S" H: v) f: `* n, M
离子抑制色谱法:ion suppression chromatography,ISC Z9#,uy 6 }% ]7 x& }$ X. I2 S2 j- M3 w; G6 {
离子色谱法:ion chromatography,IC p{wHqu+ 5 ]) m, W0 _7 }& i
手性色谱法:chiral chromatography,CC < _{;cg- 4 b' v+ h# r8 f, ]
环糊精色谱法:cyclodextrin chromatography,CDC T'(MTLg} : e* x% f8 K0 o* ?" y( U$ D
胶束色谱法:micellar chromatography,MC |e~pxkB
, o3 d% }# U9 t9 a' Y2 f亲和色谱法:affinity chromatography,AC Dg!i|PeU(
J3 j9 k# Y7 [! D固定相:stationary phase $zlk@3=O " S1 ]. r# D" A0 R1 U% N' Z
化学键合相:chemically bonde phase 3 7YacU^
& u+ C8 o/ \4 |' A封尾、封顶、遮盖:end capping "r,rET:r
3 q, M) a, U, u3 `* z$ {$ I, i手性固定相:chiral stationary phase,CSP ,/NJcjg_b 3 k2 F- Z7 g* U3 u& x# _/ V& C
恒组成溶剂洗脱:isocraic elution 7*i"< % X0 a& o. y$ \* O6 t3 p5 u M9 N
梯度洗脱:gradient elution m o|O`UG\ 0 N5 B3 {) c4 o" n! s. w) ?" U
紫外检测器:ultraviolet detector,UVD S'IJ,2#P\ . b" Q# w/ Z* E ?% |$ x# ^
荧光检测器:fluorophotomeric detector,FD Upk#M6rNU ; G) p' p9 @, O t
电化学检测器:ECD =2D+L\vE 3 r! N) m5 T4 ], @3 f0 P9 A
示差折光检测器:RID >A4WCU1 4 n/ ]/ L d2 N6 c
光电二极管检测器:photodiode array detector ,DAD `[W? @t ( C/ j. l' H' ^) D6 ^
三维光谱-波谱图:3D-spectrochromatogram bpw7p;l
0 L* r& r2 [* m2 w+ p( S# G3 k- [蒸发光散射检测器:evaporative light scattering detector,ELSD &^!P 3Z ( y" I, t; Q$ n. `; p) F s! n% e# d
安培检测器:ampere detector,AD xrcV~ ' ]$ @) y# Q4 }8 g4 g6 w6 M
高效毛细管电泳法:high performance capillary electrophoresis,HPCE [YHyEG1 3 m+ B. N$ }( c
淌度:mobility t;uxHyo` # V/ `( [6 n- P0 s7 }
电泳:electrophoresis Fkz0i!0" $ W6 L3 {: p* c: b! ^! p' M
电渗:electroosmosis Y+7~8FHf ! [! \% d$ k; t4 V; }
动力进样:hydrodynamic injection M~!"|zX
$ }' q% _2 B& h7 F电动进样:electrokinetic injection xS M`&+Y7 - I! _1 j! ?" d0 E. I+ Y
毛细管区带电泳法:capillary zone electrophoresis,CZE brO@y/_ 5 K4 _1 ~, d* U! i D: C3 y
胶束电动毛细管色谱:micellar electrokinetic capillary chromatography,MECC 1*>d3 ( i1 T' J0 N- i' P+ d
毛细管凝胶电泳:capillary gel electrophoresis,CGE V4VSf9 # Z7 i# G1 Z/ j5 }7 A
筛分:sieving o *)TraU
" f/ @" K1 t2 L7 H3 N$ C2 TspT,t " U7 S- k, ~& _" f- t5 ?$ C
绪论 (?-Z\?t}, : [6 C* v. d0 ]( e! b4 V
释药系统(drug delivery system,DDS) s]4nHE " a8 y7 Q B5 {- `7 j
中国药典(Chinese Pharmacopoeia,ChP) sH-TpY [|
/ @- u' z" T* p1 u* A, u N美国药典(The United States Pharmacopoeia,USP) S*rX%g/1s : X8 P1 p; @6 [4 _1 k& s' F8 @# [
美国国家处方集(The National Formulary,NF) ^BWj/Ty'
7 w3 D6 A6 N: j9 K5 e英国药典(British Pharmacopoeia,BP) {*_0|Oql #
3 u! T% @( W) r$ E欧洲药典(European Pharmacopoeia,Ph.Eup) d~ajs'L;5
t3 r% Y% c5 E( {+ p国际药典(The International Pharmacopoeia,Ph.Int) @Fhd>m 9 B9 [3 b! n! J9 {: n
良好药品实验研究规范(Good Laboratory Practice,GLP) ;7=`y|
& a: I; Z% I0 i& p1 P0 R良好药品生产规范(Good Manufacture Practice,GMP) ]qFIED
; u5 S" W2 p9 p# r0 \- M8 Q良好药品供应规范(Good Supply Practice,GSP) %q!1M-8 9 f) R0 i; H' P
良好药品临床试验规范(Good Clinical Practice,GCP) $JLf]9[N
$ V& }/ }$ O! `* t$ |$ J分析质量管理(Analytical Quality Control,AQC) ' T TQ
# ^; _" _+ G9 Y T, _: o第1章 药物的鉴别试验 qR0<A3WY
2 u6 d4 z2 ]) D3 O9 {! U药物的鉴别试验identification test D.r 6w9o
* }; P, ^3 m6 H. }6 O一般鉴别试验general identification test H[ +&fh3x
( K5 R, Y8 K" ^! J, O: K3 U专属鉴别试验specific identification test 8K9\$n , r0 h' G/ q7 T
灵敏度sensitivity >rnFMG d- _( X- n6 F3 c. L
最低检出量minimum detectable quantity Cx1@kc]o* + c0 ~6 C1 C$ J/ K- v y2 \
最低检出浓度minimum detectable concentration a^uwwR ]
Z$ E; O+ k, W: C$ q7 C! W第2章 药物的杂质检查 I$qb;F
, V+ g; H) X f( o" S巯基醋酸mercaptoacetic acid D=/Dfs8Z
4 }$ T& a. a8 _2 r2 u古蔡Gutzeit p^6qlmS
% Y( a7 B3 U. L3 ?# i二乙基二硫代氨基甲酸银siliver diethyldithio-carbamate 1{&(y4&w
^# n/ q# _" X硫酸灰分sulphated ash 3Q["yZ?O
! i j8 l& D( a. p% f; {炽灼残渣residue on ignition O),x&z}O
' O) y* l* @% N! p$ I) j热重分析法thermogravimetric analysis,TGA ZmkaL u Q
' u: [7 k- l9 I- g差示热分析法differential thermal analysis,DTA 9gYC& QdI 8 p2 o7 ]1 M O. R7 ^* @1 R
差示扫描量热法differential scanning calorimetry,DSC +kqNZ|8fX`
7 a) U* {$ G! \4 G! |1 l碱性酒石酸铜试验Fehling’s reagent m1%Q - }/ Q; `1 ?$ \" W9 F8 @
异红紫酸盐isopurpurate qX2o}W 0 _- X% u D0 Y6 l/ E" c: f" Q4 n
2,3-二氨基萘2,3-diaminonaphthalene ?@I> jb
6 o4 z+ w4 Q$ x4,5-苯并苯硒二唑4,5-benzopiazselenol : +S>8
# `, T, \* Y! C+ h6 `5 I第三章 定量分析样品前处理与测定方法的效能指标 GshLyN:g 1 x" @! l. m" H7 k
汞齐化法amalgamation method *W1I~nV* % T& v; b: v8 \6 ]
氧瓶燃烧法oxygen flask combustion method <30rB6Glo * G9 Q2 [: H. p- {( ^
葡萄糖醛酸甙glucuronides ):QWG$
- ?: I4 F8 F( `硫酸酯sulphates fq ])#
. I0 {4 X+ _; p血浆plasma [-!h>@f"G
7 B: f( [2 A# ] U& \血清serum f(\^i ,K : m( A& ^' @9 D( s/ o, `
全血whole blood Gx Nn? r : V4 y& v2 ]! b5 r( Q
治疗药物浓度监测therapeutic drug monitoring,TDM ?e`,t,k5
. r; J4 T9 y* V5 }- {3 U; L结合bound jIIezJ% % j$ U0 U! a( d/ l* ?0 @
游离free ;z[I;c%
( M7 s& y# E& \& Z3 R缀合物conjugate xYV >X
5 q8 B: c" a! M液-液提取法liquid-liquid extraction,LLE cUzK/J@bVK K; ]/ X- y0 ^! C
离子对试剂ion pair reagent h9{N1G\,
& _0 k! x% y% h Z& u离子对提取法ion pair extraction method Ij<4
: @7 k# B, O# {! f* x反离子counter ?RSWH=lI,_ . z* I0 ^! Q* ^3 G! O$ a
液-固提取法liquid-solid extraction LSE }^-uv;d\ 4 @8 v8 \' V+ W' K7 t7 @* n4 d. f
半自动样品制备系统advanced automated sample processor,AASP eJD0 f-1p * b( J) e$ e0 F
烷基化alkylations JS["b* ! v# Y2 |8 B3 I7 K
酰基化acylations l_3rD:b_
1 K% o. {8 n! r硅烷化silylations D!%Ca^#v % L) R9 b5 C' [+ a; ^: X4 y
精密度precision >WaF-Z /qL ! g- s, f$ ]9 F+ g" q7 c# |5 ^
标准差standard deviation,SD orS =nNjz=^ ' L: G) l+ `: ?& _+ p" v0 S! h$ `
相对标准差relative standard deviation,RSD m}(F
1 N% _2 }/ [' f4 n变异系数coefficient of variation,CV Ip{IB~w 3 V7 i$ W, N0 h' R4 G$ ^3 j
批内精密度within-run precision v{4e@$ 4 a+ @' e/ s) W6 h3 O( Z7 ]6 R
日内精密度within-day precision qW7c*xY]>
: d/ L" P; O* k, E2 i4 ^批间精密度between-run precision ~|m jX_" * z) H% i H5 o; }4 I5 z: ^
日间精密度day to day precision rJF%zcJ*@ * t% k+ v! k1 H i
准确度accuracy n)v@W6+(
( Q; G5 t: `; Y# F定量限limit of quantitation,LOQ j:.F"+;
R' t5 v8 ^5 t2 R" l" D+ k/ S检测限limit of detection,LOD ';}~8{9%{n
% `1 p# {! P4 X" L选择性selectivity cgi^7Z_&
* Z9 x( m5 |: v( K& m专属性specificity 49J6 7U 5 V9 g3 Y) {8 p9 a0 V
线性与范围linearity and range {Q)e,*( - i+ A8 F6 h# Z1 F
重现性ruggedness YIR av'
* {, v/ h2 ^. U耐用性robustness NYA^xh 4 S) H) G, G+ I! a# m4 L
散布图scatter diagram ;>kacf[S % w; ~6 Q$ |$ k, `) L4 z; A2 a
荧光偏振免疫测定法fluorescence polarization immunoassay,FPIA t D6%C;fP
+ `8 _( f, K. E& M6 n第4章 巴比妥类药物的分析 3$ H 0 \* X4 g) m1 X; I" k
溴化十六烷基三甲基苄铵cetyltrimethylbenzylammonium bromide,CTMA g{\.V(
- g" W: y/ l. E4 L3 o氯化四癸基二甲基苄铵Tetradacyldimethybenzylammonium chloride,TDBA 3GKwv,##Vb % q! k& Q; K/ {/ l/ W
第5章 芳酸及其酯类药物的分析 G>>U 6~ ) s& b/ w2 F/ g+ ?# J6 x5 G+ C
苯甲酸及其钠盐benzoic acid and sodium benzoate I<s!> tM
" c; w1 h6 x8 }2 ]布美他尼bumetanide zSj>pBe
0 T% g9 G: ]: \$ c2 h' b羟苯乙酯ethylparoben e|3Qw{ !L, y; a* |* R4 h' R" T7 J" o& f; u
丙磺舒probenecid odNkG:R.
5 P' ~! k+ ^2 w' b5 [0 w3 h酚黄乙胺etamsylate "r!j} `:
. i3 l `8 Q3 _6 w2 m4 l7 ?第6章 胺类药物的分析 .s8]]CR ( u6 ?& l6 k' u2 q! E% u
第七章 杂环类药物的分析 ugP jydb
% O- E3 E; h6 t# I8 j, K% w! S7 L5 l二硝基氯苯反应Vongerichten反应 D,R{vjP-
4 ], {7 Q- e" Z1 W戊烯二醛反应K?nig反应 :V)mM7|& & : Z0 W7 u% I" z8 t4 C
第8章 生物碱类药物的分析 } MGfq/L
9 _1 U) j3 \" M# }1 e生物碱alkaloids g |52bH 6 y5 z; a/ J) j/ v& Z/ x
阿片gum opium 06H% JNg
2 r5 T; Y' x+ D H5 @扫尾剂tailing-suppressing reagent zrs-NR#R 5 w9 T+ ~' W# }3 |
蒂巴因thebaine kkmC/6H # R5 f. I+ b( f; l. S j' f
诺司卡品noscapine 3'32moev/
$ J3 E6 g: c5 Q2 r. ^- X竞争离子competing ions 3Nu*#10#x{
7 u+ F E6 N/ k1 I2 |亲脂性lipophicity KS?3_*
" y2 H' o7 {( G, ^8 V0 A6 s拖尾因子tailing factor Fq~Ekm%oM
% X7 T |7 g! k, y* }* j金刚烷adamantane e Y 1 7Tu
4 D6 d) |) d+ E/ H c+ T第9章 维生素类药物的分析 3URM !va 6 G" L1 g# H* K1 s" \
维生素vitamin |
|